CURRENT CONTROL OF GRAY IRON TENSILE PROPERTIES

By

The Quality Control Committee

of the

Cast Iron Division

of the

American Foundrymen’s Society

 

Principle Author

Roy W. Lobenhofer

Lobenhofer Consulting, Inc.

 

“How good does control need to be?” is a question that many technical foundrymen ask themselves. While improved control is always desirable, in reality every foundry must deal with limited resources. It’s important to spend those resources on improving the control of variables that will most significantly benefit the operation. Realizing the importance of this question about degree of control, the Quality Control Committee of the Cast Iron Division of the American Foundrymen’s Society decided to try to determine what degree of control is being achieved in today’s iron foundries.

As one of the variables every iron foundry must control is the tensile strength, it was decided to start with that variable. A survey form was developed which asked foundries to report the only the degree of variability they experienced in tensile strength. The foundries were requested to report only their degree of variability to avoid possible concerns about proprietary information. The form also requested information about the operations that might effect the variability tensile strength. It was decided that in order to make the information consistent that the information would only be sought on class 30 gray iron, the most commonly poured grade of gray iron. The survey and cover letter that was sent with it are attached as appendix A.

 Using the information in the AFS computer, the survey was sent to over 2000 technical people in gray iron foundries. Unfortunately, only 32 operations responded. As poor as that return was, it would have been far worse, if committee members had not sent personal requests to foundries.

Even with the limited response, interesting information was obtained from the survey. Obviously, the primary information sought was the variability being experienced in tensile strength. The survey revealed that the average standard deviation to be 2256 psi. The maximum and minimum reported were 3845 and 1120 respectively.

One of the suspected contributing factors to the variability was whether the tensile testing was done in-house or by commercial laboratory. 15 of the operations indicated that they used commercial laboratories. The average standard deviation of the tensile for those operations was 2330. The 17 foundries indicating they performed their own tensile testing had an average standard deviation from their tensile testing of 2190 psi.

 

Another factor investigated to see if it would have an effect on tensile control was melting method. Table 1 and Figure 1 indicate the survey results did show that melting method affected the results.

Linear regression analyses were performed comparing all of the quantifiable data to the standard deviations. The correlation coefficient measures how well the developed formula explains the variation. The variable that showed the best correlation was sulfur. Figure 2 shows the scatter of the sulfur standard deviation in relation to the tensile standard. There were 24 foundries that reported sulfur standard deviations and the correlation coefficient of the equation .534.

The next highest correlation was .282 from the equation relating the standard deviation of the silicon as determined by thermal analysis to the standard deviation of the tensile strength.

It was believed that there would be a high correlation between the amount of variation experienced in the hardness readings and the tensile strength. The correlation coefficient actually found .167. The scatter diagram of that relationship is shown in figure 3.

Discussion of Findings

Limited Response

The limited response to the survey was naturally disappointing. It was believed by the members of the committee that the information requested would be readily available in most of today’s iron foundries and a good response was expected from survey. Previous committee survey’s sent using the AFS database have had far higher returns than this. There are a number of possibilities for the poor return rate.

1)       Obviously, a poorly worded survey form can frustrate the person trying to fill it out and the form is likely to end up being thrown out. On occasion people developing surveys can fall into the trap of knowing exactly what they mean because they had worked on it for so long, but it can be very confusing to the person trying to fill it out. In order to avoid this happening, the committee, after finishing developing the form had it sent, to colleagues who were not involved with its development to see if there were any misunderstandings. As the colleagues had no problem interpreting the survey, the committee felt that had eliminated the concern. 

2)       Another common problem with surveys is that they get sent to the wrong people. As the AFS database used for the surveys similar to this that had far greater returns than this, it would seem that this would not be a viable reason for the poor return on this one.

3)       It is well known that surveys requiring the responders to spend a great deal of effort developing the information asked for do not get high responses. With the computers in use in foundries today, the emphasis placed on statistical tracking, and the importance of control of variables, it was believed that most foundries would have easy access to the desired information. Investigations outside of the committee have shown that belief was very likely erroneous. The information was not readily available in a number of foundries. That being the case, it is easy to understand that the people asked to respond would not believe seeing the results of the survey would not be beneficial to them.

 

Overall Results

The overall “average” standard deviation of the tensile strength shown from the survey results may be better/lower than is the real “average” of all foundries producing class 30 gray iron. As indicated above the low return of surveys may have been caused because not many foundries track the variability of the tensile strength. If that is the case, then it is almost certain the foundries that are not tracking it are not placing a great deal of emphasis on controlling it. Simple logic would then lead to the conclusion, that there would be a likelihood that such foundries would have a higher standard deviation. 

In-house Testing versus Commercial Laboratories

While the average of the tensile standard deviations of the foundries that did there own tensile testing was lower than those of the foundries that used commercial laboratories, the difference was not statistically significant. While one would assume that the results obtained from a commercial laboratory would be less variable than those done by a foundry, there are a number of reasons why this may not be the case in reality.

1)       The foundries that can afford the capital equipment to do there own tensile testing would tend to be the larger operations. Such larger operations would be more likely to have sophisticated controls in place that could lead to better control of the tensile properties.

2)       When tensile testing is done in-house, it is easier to retest questionable results. Naturally, eliminating “flyers” from the data will reduced the resulting standard deviations.

3)       Commercial laboratories typically test a wider range of materials than in-house laboratories. This should allow the in-house testing procedures to be fine tuned to produce less variable results.

Melting Procedures

As there was only one reporting foundry that used an arc furnace, there can be no statistical significance attributed to its having the lowest average standard deviation. The differences in averages among the other types of melting are all statistically significant at over a 90% confidence level.

Once again there is logic to these results. The duplexing melting system is usually associated with larger operations that would be expected to have better control equipment. The balancing effect of duplexing furnaces also should improve control. While the cupola and induction furnace both melt iron, the chemical reactions that are part of the cupola melting usually equate to more difficult control.

Linear Relationships

The information from performing the regression analyses was confusing. Regression analyses were performed comparing the standard deviations all available variables to the standard deviation of the tensile strength. The results did not provide significant insights.  The lack of a strong relationship between the standard deviations of the hardness readings and the tensile strength (correlation coefficient of .167) was as surprising as the good correlation (correlation coefficient of .533) between sulfur.

Conclusions 

It’s difficult to draw any significant conclusions from such a small response. Perhaps the cause of the small response is the most significant factor of this entire exercise. It is theorized that iron foundries are not tracking their degree of control of their tensile strength. If they are not tracking their control on a variable that is specified, it can be deduced that they would also not track other non-specified variables in the operation.

The reduction of process variation has been shown to be the key to improved quality performance and has been extolled by the giants of the quality movement such as Demming; however, with these results it is appropriate to conclude with a quote from Peter Drucker: 

“Don't measure it and your people know you're not serious about delivering it.”

  

Furnace

Average Standard Deviation

Number

Cupola

2720

10

Induction

2315

15

Duplex

1465

6

Arc

1459

1

Table 1 – Melting Method


Figure 1

Figure 2



Figure 3

AFS CAST IRON DIVISION’S QUALITY CONTROL COMMITTEE’S

SURVEY OF IRON CONTROL

STANDARD DEVIATIONS OF CLASS 30 TENSILE TESTS

NUMBER OF TESTS REPRESENTED IN SAMPLE _________ TIME SPAN ________

STD. DEV. OF TENSILE TESTS _______

STD. DEV. OF BHN OF TEST BARS ______

RESULTS FROM ______ IN HOUSE TESTING _____ COMMERCIAL LAB

MELTING - CUPOLA ____ INDUCTION ____ DUPLEX ______

IN HOUSE THERMAL ANALYSIS RESULTS

STD. DEV. OF C _____

STD. DEV OF Si

OTHER CHEMICAL ANALYSIS

SOURCE _________________________

 

 

ELEMENT

 

STD. DEV.

 

ELEMENT

 

STD. DEV.

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

PLEASE LIST STANDARD DEVIATIONS OF ANY OTHER TESTS WHICH YOU DEEM SIGNIFICANT ON AN ADDITIONAL SHEET.

 

OPTIONAL:

CONTACT PERSON’S NAME _________________

COMPANY NAME __________________________

TELEPHONE NUMBER ____________________

PLEASE FAX RESULTS TO 847.806.1229


COVER LETTER

Dear Foundryman:

The AFS Cast Iron Division’s Quality Control Committee (5-J) is trying to quantify the control being exercised in today’s iron foundry. In order to begin this endeavor it was decided to look at the control being exercised in producing the class 30 gray iron test bars. To help us in this matter, we are requesting that you fill out the enclosed form regarding the standard deviation of your test results for a number of consecutive tests and a little information about how the testing was accomplished.

 

We realize that no one will want to release information that might be sensitive to their operation; therefore, we are only asking questions regarding the degree of control being exercised. We don’t expect you to run any special tests. We hope that all of the information will merely come from your records.

 

We would like the tensile tests you report to be consecutive (no fair picking out only the good ones) and a minimum of twenty-five test bar results. If you don’t track the chemistry information directly with your test bar results, we ask that you make the report of that information covering your data for the same time period instead of just using the same number of tests.

While it isn’t necessary, we would like you to include your name and telephone number so that a follow up can be made if there is any clarification of information that needs to be done.

 

It is our hope to turn this information into a Modern Casting article that will give you either bragging rights with your management about what a good job you’re doing controlling your iron or ammunition to get what you need to improve control.

If you have any questions regarding this activity or the other activities of the Cast Iron Quality Committee, please feel free to call me at the number listed below.

 

Sincerely,

 

 

 

 

 

Roy Lobenhofer

847.806.1212

On behalf of the

Cast Iron Division’s

Quality Control Committee


RAW DATA

Foundry

# Tests

Time Span - Yr

Std Dev Tensile

Std Dev BHN

1=Commerical Lab 2=in house

Melting        1=cupola   2=Induction     3=duplex

Thermal C

Thermal Si

Chem Source

C

Si

a

46

0.083333

1852

4

2

3

0.012

0.022

Leco/Spec

0.015

0.035

b

25

0.333333

3671

4.5

2

1

0.058

0.108

spec

na

0.2

c

67

0.083333

1250

5

2

3

0.025

0.048

spec

x

x

d

56

0.166667

2800.1

5.2876

2

2

0.0825

0.11973

?

x

x

e

25

0.016438

2990

5.8

2

1

0.02

0.05

x

x

x

f

35

0.083333

1120

6

2

3

0.017

0.039

spec

x

x

g

41

0.10137

1300

6.2

2

1

x

x

Leco/Spec

0.04

0.074

h

39

0.035616

1459

6.43

1

Arc

0.046

0.049

spec

x

x

I

30

0.038356

1602

6.464

2

2

x

x

spec

0.0466

0.048

j

43

0.054795

1738.5

6.52

1

3

0.033

0.124

spec

x

x

k

25

0.117808

1590

6.86

2

2

0.003

0.002

x

x

x

l

66

0.083333

1522

6.9

2

3

0.028

0.047

spec

x

x

m

25

0.208333

3845.2

7.88

2

2

x

x

Leco/Spec

0.07

0.09

n

63

0.083333

1305

8

2

3

x

x

?

0.013

0.025

o

27

0.583333

1668

8

1

1

0.04

0.07

spec

x

x

p

59

0.25

2078

8.1

1

2

x

x

spec

0.074

0.077

q

33

0.083333

2708

8.6

1

1

0.04

0.12

spec

0.056

0.111

r

50

0.5

1964.854

9.203

1

2

0.022

+

spec

0.139

0.046

s

46

0.083333

2050

9.9

2

2

0.033

0.047

spec

0.063

0.096

t

25

0.08

2132.2

10

1

2

0.1552

na

spec

na

0.1662

u

26

0.083333

2300

10

1

2

0.027

0.025

spec

x

x

v

38

0.084932

1905.84

10.6

1

2

0.02

0.06

?

x

x

w

25

0.583333

2466.7

10.8

1

2

0.042

0.061

Com. Spec

x

x

x

741

1.25

2418

11.23

1

1

na

na

in house

0.0262

0.1041

y

25

0.076923

3158

12.2

1

2

0.038

0.106

Spec

x

x

z

31

0.125

3031.85

12.98

1

1

0.02

x

spec

x

0.08

aa

453

0.125

3490

13.1

2

1

x

x

Leco/Spec

0.024

0.05

ab

328

1.416667

2928

13.9

2

2

0.06

0.11

spec

x

x

ac

29

0.083333

2290

14.7

2

2

0.04

0.06

spec

0.084

0.09

ad

24

0.041096

3059

15

1

1

0.05

0.07

x

x

x

ae

22

0.5

1618.6

x

2

2

0.0347

0.0362

x

x

x

af

100

1

2865

x

1

1

0.03

0.04

x

x

x

 


 

Foundry

Mn

S

P

Cr

Ni

Cu

Al

Ti

V

Sn

Mo

Sb

Nb

Zr

a

0.033

0.004

0.003

0.011

0.002

0.009

0.001

0.006

x

0.002

0.002

na

na

na

b

0.04

0.022

0.007

0.007

0.01

0.07

na

na

na

na

na

na

na

na

c

0.029

0.005

0.001

0.018

0.003

0.01

x

0.001

x

x

0.001

x

x

x

d

0.0324

x

x

x

x

x

x

x

x

x

x

na

na

na

e

x

x

x

x

x

x

x

x

x

x

x

na

na

na

f

0.02

0.004

0.004

0.012

0.005

0.016

x

0.002

x

x

0.003

x

x

x

g

0.026

0.004

0.0028

+

+

0.014

+

0.0035

+

+

+

na

na

na

h

0.017

0.003

0.004

0.013

x

0.009

x

0.0014

x

x

x

x

x

x

I

0.0254

0.0034

0.0015

0.0043

0.0017

0.026

0.0022

0.0011

0.0033

x

0.0025

na

na

na

j

0.0588

0.0078

0.0024

0.0079

0.0055

0.0187

0.0005

0.0031

x

0.0023

0.0048

0.0012

na

na

k

x

x

x

x

x

x

x

x

x

x

x

na

na

na

l

0.019

0.006

0.002

0.016

0.004

0.012

x

0.001

x

x

0.004

x

x

x

m

x

x

x

x

x

x

x

x

x

x

x

na

na

na

n

0.026

0.003

0.002

0.013

x

0.015

x

0.0009

0.001

0.0006

0.006

0.0013

0.001

0.0005

o

0.03

0.01

0.003

0.02

0.006

0.03

x

x

x

0.002

x

x

x

x

p

0.019

0.005

0.005

x

x

0.025

x

x

x

0.007

0.017

na

na

na

q

0.037

0.014

0.012

0.0095

0.005

0.0148

0.0065

0.003

*

0.02

0.003

x

x

x

r

0.019

0.0074

0.0013

0.011

0.0191

0.0541

0.0018

0.0007

na

0.0025

0.0306

na

na

na

s

0.05

0.014

0.005

0.07

0.01

0.1

0.003

0.006

0.003

0.003

0.02

x

x

x

t

0.0686

0.0088

0.0171

na

na

0.1048

na

na

na

na

na

na

na

na

u

0.021

0.008

0.047

x

x

x

x

x

x

x

x

na

na

na

v

0.06

0.01

0.01

0.03

0.03

0.07

x

x

x

x

x

na

na

na

w

0.047

0.01

0.0078

0.014

x

x

x

x

x

x

x

na

na

na

x

0.036

0.0139

0.0134

0.0483

0.0182

0.1024

0.0053

0.0034

0.007

0.0121

0.0039

na

na

na

y

0.08

0.009

0.004

0.022

0.047

0.059

0.001

0.002

0.001

0.003

0.038

na

na

na

z

x

x

x

x

x

x

x

x

x

x

x

na

na

na

aa

x

0.0099

0.0111

0.01

x

0.028

x

0.001

x

0.0031

0.0057

x

x

x

ab

x

x

x

0.013

0.0053

0.042

x

x

x

x

0.019

na

na

na

ac

0.07

0.005

0.009

0.06

0.04

0.09

0.002

0.003

0.002

0.003

0.002

x

x

x

ad

x

x

x

x

x

x

x

x

x

x

x

na

na

na

ae

x

x

x

x

x

x

x

x

x

x

x

na

na

na

af

x

x

x

x

x

x

x

x

x

x

x

na

na

na